HJ 605-2011 土壤和沉积物挥发性有机物的测 吹扫捕集/气相色谱-质谱法,该方法原理是:样品中的挥发性有机物经高纯氦?或氮?吹扫富集于捕集管中,将捕集管加热并以高纯氦气反吹,被热脱附出来的组分进入气相色谱并分离后,用质谱仪进行检测。通过与待测目标物标准质谱图相比较和保留时间进行定性,内标法定量、/p>
下表给出了目标物的检出限、测定下限和最小相对响应因子、/p>
| 序号 | 目标物中文名?/strong> | 目标物英文名?/strong> | 检出限 (μg/kg) |
测定下限 (μg/kg) |
最小相寸br/>响应因子 |
| 1 | 二氯二氟甲烷 | dichlorodifluoromethane | 0.4 | 1.6 | 0.1 |
| 2 | 氯甲烶/td> | chloromethane | 1.0 | 4.0 | 0.1 |
| 3 | 氯乙?/td> | chloroethene | 1.0 | 4.0 | 0.1 |
| 4 | 溴甲烶/td> | bromomethane | 1.1 | 4.4 | 0.1 |
| 5 | 氯乙烶/td> | chloroethane | 0.8 | 3.2 | 0.1 |
| 6 | 三氯氟甲烶/td> | trichlorofluoromethane | 1.1 | 4.4 | 0.1 |
| 7 | 1,1-二氯乙烯 | 1,1-dichloroethene | 1.0 | 4.0 | 0.1 |
| 8 | 丙酮 | acetone | 1.3 | 5.2 | 0.1 |
| 9 | 碘甲烶/td> | iodo-methane | 1.1 | 4.4 | ,/td> |
| 10 | 二硫化碳 | carbon disulfide | 1.0 | 4.0 | 0.1 |
| 11 | 二氯甲烷 | methylene chloride | 1.5 | 6.0 | 0.1 |
| 12 | 反式-1,2-二氯乙烯 | trans-1,2-dichloroethene | 1.4 | 5.6 | 0.1 |
| 13 | 1,1-二氯乙烷 | 1,1-dichloroethane | 1.2 | 4.8 | 0.2 |
| 14 | 2,2-二氯丙烷 | 2,2-dichloropropane | 1.3 | 4.2 | ,/td> |
| 15 | 顺式-1,2-二氯乙烯 | cis-1,2-dichloroethene | 1.3 | 4.2 | 0.1 |
| 16 | 2-丁酮 | 2-butanone | 3.2 | 13 | 0.1 |
| 17 | 溴氯甲烷 | bromochloromethane | 1.4 | 5.2 | ,/td> |
| 18 | 氯仿 | chloroform | 1.1 | 4.4 | 0.2 |
| 19 | 二溴氟甲烶/td> | dibromofluoromethane | ,/td> | ,/td> | ,/td> |
| 20 | 1,1,1-三氯乙烷 | 1,1,1-trichloroethane | 1.3 | 5.2 | ,/td> |
| 21 | 四氯化碳 | carbon tetrachloride | 1.3 | 5.2 | 0.1 |
| 22 | 1,1-二氯丙烯 | 1,1-dichloropropene | 1.2 | 4.8 | ,/td> |
| 23 | ?/td> | benzene | 1.9 | 7.6 | 0.5 |
| 24 | 1,2-二氯乙烷 | 1,2-dichloroethane | 1.3 | 5.2 | 0.1 |
| 25 | 氟苯 | fluorobenzene | ,/td> | ,/td> | ,/td> |
| 26 | 三氯乙烯 | trichloroethylene | 1.2 | 4.8 | 0.2 |
| 27 | 1,2-二氯丙烷 | 1,2-dichloropropane | 1.1 | 4.4 | 0.1 |
| 28 | 二溴甲烷 | dibromomethane | 1.2 | 4.8 | ,/td> |
| 29 | 一溴二氯甲烶/td> | bromodichloromethane | 1.1 | 4.4 | ,/td> |
| 30 | 4-甲基-2-戊酮 | 4-methyl-2-pentanone | 1.8 | 7.2 | ,/td> |
| 31 | 甲苯-D8 | toluene-D8 | ,/td> | ,/td> | ,/td> |
| 32 | 甲苯 | toluene | 1.3 | 5.2 | 0.4 |
| 33 | 1,1,2-三氯乙烷 | 1,1,2-trichloroethane | 1.2 | 4.8 | ,/td> |
| 34 | 四氯乙烯 | tetrachloroethylene | 1.4 | 5.6 | 0.2 |
| 35 | 1,3-二氯丙烷 | 1,3-dichloropropane | 1.1 | 4.4 | ,/td> |
| 36 | 2-己酮 | 2-hexanone | 3.0 | 12 | ,/td> |
| 37 | 二溴氯甲烶/td> | dibromochloromethane | 1.1 | 4.4 | 0.1 |
| 38 | 1,2-二溴乙烷 | 1,2-dibromoethane | 1.1 | 4.4 | ,/td> |
| 39 | 氯苯-D5 | chlorobenzene-D5 | ,/td> | ,/td> | ,/td> |
| 40 | 氯苯 | chlorobenzene | 1.2 | 4.8 | 0.5 |
| 41 | 1,1,1,2-四氯乙烷 | 1,1,1,2-tetrachloroethane | 1.2 | 4.8 | ,/td> |
| 42 | 乙苯 | ethylbenzene | 1.2 | 4.8 | 0.1 |
| 43 | 1,1,2-三氯丙烷 | 1,1,2-trichloropropane | 1.2 | 4.8 | ,/td> |
| 44 | ?二甲?/td> | m,p-xylene | 1.2 | 4.8 | 0.1 |
| 45 | ?二甲?/td> | m,p-xylene | 1.2 | 4.8 | 0.1 |
| 46 | ?二甲?/td> | o-xylene | 1.2 | 4.8 | 0.3 |
| 47 | 苯乙?/td> | styrene | 1.1 | 4.4 | 0.3 |
| 48 | 溴仿 | bromoform | 1.5 | 6.0 | 0.1 |
| 49 | 异丙?/td> | isopropylbenzene | 1.2 | 4.8 | 0.1 |
| 50 | 4-溴氟?/td> | 4-bromofluorobenzene | ,/td> | ,/td> | ,/td> |
| 51 | 溴苯 | bromobenzene | 1.3 | 5.2 | ,/td> |
| 52 | 1,1,2,2-四氯乙烷 | 1,1,2,2-tetrachloroethane | 1.2 | 4.8 | 0.3 |
| 53 | 1,2,3-三氯丙烷 | 1,2,3-trichloropropane | 1.2 | 4.8 | ,/td> |
| 54 | 正丙?/td> | n-propylbenzene | 1.2 | 4.8 | ,/td> |
| 55 | 2-氯甲?/td> | 2-chlorotoluene | 1.3 | 5.2 | ,/td> |
| 56 | 1,3,5-三甲基苯 | 1,3,5-trimethylbenzene | 1.4 | 5.6 | ,/td> |
| 57 | 4-氯甲?/td> | 4-chlorotoluene | 1.3 | 5.2 | ,/td> |
| 58 | 叔丁基苯 | tert-butylbenzene | 1.2 | 4.8 | ,/td> |
| 59 | 1,2,4-三甲基苯 | 1,2,4-trimethylbenzene | 1.3 | 5.2 | ,/td> |
| 60 | 仲丁基苯 | sec-butylbenzene | 1.1 | 4.4 | ,/td> |
| 61 | 1,3-二氯?/td> | 1,3-dichlorobenzene | 1.5 | 6.0 | 0.6 |
| 62 | 4-异丙基甲?/td> | p-isopropyltoluene | 1.3 | 5.2 | ,/td> |
| 63 | 1,4-二氯?D4 | 1,4-dichlorobenzene-D4 | ,/td> | ,/td> | ,/td> |
| 64 | 1,4-二氯?/td> | 1,4-dichlorobenzene | 1.5 | 6.0 | 0.5 |
| 65 | 正丁基苯 | n-butylbenzene | 1.7 | 6.8 | ,/td> |
| 66 | 1,2-二氯?/td> | 1,2-dichlorobenzene | 1.5 | 6.0 | 0.4 |
| 67 | 1,2-二溴-3-氯丙烶/td> | 1,2-dibromo-3-chloropropane | 1.9 | 7.6 | 0.05 |
| 68 | 1,2,4-三氯?/td> | 1,2,4-trichlorobenzene | 0.3 | 1.2 | 0.2 |
| 69 | 六氯丁二?/td> | hexachlorobutadiene | 1.6 | 6.4 | ,/td> |
| 70 | 萗/td> | naphthalene | 0.4 | 1.6 | ,/td> |
| 71 | 1,2,3-三氯?/td> | 1,2,3-trichlorobenzene | 0.2 | 0.8 | ,/td> |
注:没有规定最小相对响应因子的化合物,其最小相对响应因子不作限值规定、br/>