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CAS: 574-98-1
分子式: C10H8BrNO2
分子量: 254.09
熔点: 81-84℃
中文名称: 
N-(2-溴乙基苄酰胺)
β-溴乙基邻苯二甲酰亚胺
N-β-溴乙基酞酰亚胺
邻苯二甲酰溴乙亚胺
N-(2-溴乙基)邻苯二甲酰亚胺
英文名称: 
2-(2-bromoethyl)-1h-isoindole-3(2h)-dione
n-(2-bromoethyl)phthalimide
-Bromoethylphthalimide
N-Bromoethylphthalimide
性质描述: 白色针状晶体。熔点82-83.5℃。易溶于乙醚,在热水中分解。
生产方法: 邻苯二甲酸酐经缩合、溴化而得:在反应锅内投入邻苯二甲酸酐,缓缓加入乙醇胺,加热至110℃蒸去水分,再真空干燥2h。于110-120℃滴加三溴化磷,加毕,保温搅拌1.5h。冷至80℃,放料到碎冰中,分解多余的三溴化磷,静置过夜,得结晶,离心甩干,再用乙醇重结晶,于60℃左右干燥,得成品。
用途: 药物中间体。
推荐供应商
货号品牌产品名称规格包装、参考价格
N830664MACKLINN-(2-溴乙基)邻苯二甲酰亚胺95 %24元/5g;   71元/25g;   283元/100g;   1202元/500g;   咨询
储存:室温,密封
B0597TCIN-(2-Bromoethyl)phthalimide>98.0%(GC)(T)315元/25G;   935元/100G;   咨询

基本信息

纯度/分析方法>98.0%(GC)(T)
分子式/分子量C10H8BrNO2 = 254.08
外观与形状(20℃)固体
Reaxys-RN148736
PubChem物质ID87563612
SDBS (AIST Spectral DB)824
MDL编号MFCD00005902

技术规格

AppearanceWhite to Almost white powder to crystal
Purity(GC)min. 98.0 %
Purity(Argentometric Titration)min. 98.0 %
Melting point81.0 to 85.0 ℃
Solubility in hot Methanolalmost transparency

物性(参考值)

熔点82 ℃
沸点318 ℃
水溶性可溶
溶解性(可溶于)甲醇
264138J&KN-(2-Bromoethyl)phthalimide96%285元/25G;   823元/100G;   咨询

基本信息

分子式C10H8BrNO2
分子量254.08
熔点80-83
沸点318
MDL编码MFCD00005902
Beilstein148736
EINECS 编号209-379-9

安全信息

防范说明P262
WGK3
TSCA
A12164Alfa AesarN-(2-Bromoethyl)phthalimide98+%647元/25g;   2100元/100g;   6993元/500g;   咨询

应用
N-(2-Bromoethyl)phthalimide is an intermediate used in organic synthesis. It can react with phenyl magnesium bromide to get 2-(2-bromo-ethyl)-3-hydroxy-3-phenyl-isoindolin-1-one.

备注
Store in cool, dry place in a tightly sealed container. Store away from oxidizing agent.

基本信息

MDL
MFCD00005902

EINECS
209-379-9

分子式
C10H8BrNO2

分子量
254.09

熔点
80-84°

灵敏度
Ambient temperatures.

形态
Crystalline powder

溶解性
Soluble in water (224 mg/L at 25°C).

Beilstein
148736

安全信息

TSCA

C10697Alfa AesarN-(2-Bromoethyl)phthalimide97%887元/25g;   1830元/100g;   咨询

基本信息

Ref#
10697

MDL
5902

分子式
C10 H8 Br N O2

分子量
254.08

B66302Sigma-AldrichN-(2-Bromoethyl)phthalimide95%324.47元/25 G;   843.93元/100 G;   咨询

基本信息

经验(实验)分子式C10H8BrNO2
分子量254.08
Beilstein148736
EC 号209-379-9
MDL编号MFCD00005902
PubChem化学物质编号24891924
NACRESNA.22

产品性质

质量水平200
测定95%
reaction suitabilityreagent type: cross-linking reagent
mp80-83 ℃ (lit.)
SMILES stringBrCCN1C(C2=CC=CC=C2C1=O)=O
InChI1S/C10H8BrNO2/c11-5-6-12-9(13)7-3-1-2-4-8(7)10(12)14/h1-4H,5-6H2
InChI keyCHZXTOCAICMPQR-UHFFFAOYSA-N

安全信息

储存分类代码13 - Non Combustible Solids
WGKWGK 3
闪点(F)Not applicable
闪点(C)Not applicable
个人防护装备Eyeshields, Gloves, type N95 (US)
033105FluorochemN-(2-Bromoethyl)phthalimide95+%220元/10g;   220元/1g;   418元/25g;   1254元/100g;   5632元/500g;   咨询

基本信息

CAS Number574-98-1
MDL NumberMFCD00005902
Melting Point81-84℃

安全信息

图形或危害标志
危险性说明 H315: Causes skin irritation.
H319: Causes serious eye irritation.
H335: May cause respiratory irritation.
防范说明 P233: Keep container tightly closed.
P260: Do not breathe .
P261: Avoid breathing .
P264: Wash hands thoroughly after handling.
P271: Use only outdoors or in a well-ventilated area.
P280: Wear .
P302 + P352: IF ON SKIN: Wash with plenty of soap and water.
P304: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing..
P304 + P340: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P312: Call a POISON CENTER or doctor/physician if you feel unwell.
P321: Specific treatment (see relevant procedures. on this label).
P332 + P313: If skin irritation occurs: Get medical advice/ attention.
P337 + P313: If eye irritation persists: Get medical advice/attention.
P340: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P362: Take off contaminated clothing and wash before reuse.
P403: Store in a well-ventilated place.
P403 + P233: Store in a well-ventilated place. Keep container tightly closed.
P405: Store locked up.
P501: Dispose of contents/container to in accordance with local regulation .
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