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CAS: 109-64-8
分子式: C3H6Br2
分子量: 201.89
沸点: 167℃
熔点: -34-167℃
中文名称: 
1,3-二溴丙烷
三亚甲基二溴
溴化三次甲基
溴化三亚甲基
英文名称: 
,-Dibromopropane
,'-Dibromopropane
Propane,1,3-dibromo-
1,3-dibromo-propane
1,3-Dibrompropan
α,γ-Dibromopropane
ω,ω'-Dibromopropane
Trimethylendibromid
1,3-Dibromopropane
1,3-dibromo-Propane
1,3-Propylene bromide
alpha,gamma-dibromopropane
omega,omega'-dibromopropane
1,3-dibromo-propan
trimethylene bromide
trimethylene dibromide
展开更多英文名
性质描述: 无色或淡黄色液体。凝固点-34.2℃,沸点165℃(167.3℃),59-63℃(2.66kPa),55.6℃(1.33kPa),相对密度1.9822(20/4℃),折光率1.5232,闪点54℃。溶于乙醚、丙酮和氯仿,不溶于水。长时间遇热则分解,并部分转变为1,2-二溴丙烷。与水煮沸产生丙二醇。无臭,味甜,易吸潮。
生产方法: 由丙二醇与溴氢酸反应而得。先向溴氢酸中加入浓硫酸和1,3-丙二醇,然后再慢慢滴入浓硫酸,在砂浴上回流7h,然后蒸出粗品,将粗品用水洗一次,用10%硫代硫酸钠溶液洗2-3次,10%碳酸钠洗两次,分去水层,用无水氯化钙干燥。经常压分馏,收集159-168℃馏分而得成品。
用途: 作有机合成中间体。
推荐供应商
货号品牌产品名称规格包装、参考价格
D806820MACKLIN1,3-二溴丙烷99%32元/25g;   72元/100g;   176元/500g;   758元/2.5kg;   2420元/10kg;   咨询
储存:室温
状态:无色到淡黄色液体
折射率:n20/D 1.524(lit.)
D806819MACKLIN1,3-二溴丙烷98%51元/100g;   160元/500g;   709元/2.5kg;   1899元/12X500g;   咨询
储存:室温
状态:无色到淡黄色液体
折射率:n20/D 1.524(lit.)
208394J&K1,3-Dibromopropane99%126元/25ML;   255元/100ML;   901元/500ML;   咨询

基本信息

分子式C3H6Br2
分子量201.89
熔点-34
沸点167
闪点56
密度1.989
MDL编码MFCD00000255
Beilstein635662
Merck14,9713
EINECS 编号203-690-3

安全信息

图形或危害标志
提示语Warning
危险说明H226
H302
H315
H319
H411
防范说明P211
P273
P281
P305+P351+P338
P370+P378
UN号码1993
危险分类3
包装等级III
WGK2
RTECSTX8575000
TSCA
125903Sigma-Aldrich1,3-DibromopropaneReagentPlus®, 99%525.74元/50 ML;   3795.15元/1 L;   咨询

产品说明

一般描述

1,3-二溴丙烷是一种二卤代丙烷。在碳电极表面的聚合物膜中,它分别被电生液相镍 (I) 手性和镍 (I) 手性催化还原生成环丙烷和丙烯。

应用

1,3-二溴丙烷可用于制备手性孪生双阳离子离子液体 和 1,3-双(1-7′-氯-4-喹啉基-4-哌嗪基)丙烷。3

包装

1 L in glass bottle
50 mL in glass bottle

法律信息

ReagentPlus is a registered trademark of sigma-aldrich Co. LLC

基本信息

线性分子式Br(CH2)3Br
分子量201.89
Beilstein635662
EC 号203-690-3
MDL编号MFCD00000255
PubChem化学物质编号24847685
NACRESNA.21

产品性质

质量水平100
蒸汽密度7 (vs air)
产品线ReagentPlus®
测定99%
形式liquid
折射率n20/D 1.524 (lit.)
bp167 ℃ (lit.)
mp−34 ℃ (lit.)
密度1.989 g/mL at 25 ℃ (lit.)
SMILES stringBrCCCBr
InChI1S/C3H6Br2/c4-2-1-3-5/h1-3H2
InChI keyVEFLKXRACNJHOV-UHFFFAOYSA-N

安全信息

象形图GHS02GHS07GHS09
警示用语:Warning
危险声明H226 - H302 - H315 - H411
预防措施声明P210 - P233 - P240 - P273 - P301 + P312 - P303 + P361 + P353
危险分类Acute Tox. 4 Oral - Aquatic Chronic 2 - Flam. Liq. 3 - Skin Irrit. 2
储存分类代码3 - Flammable liquids
WGKWGK 2
闪点(F)129.2 °F - closed cup
闪点(C)54 ℃ - closed cup
个人防护装备Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
8.03279Sigma-Aldrich1,3-Dibromopropanefor synthesis872.8元/100 ML;   1916.59元/250 ML;   咨询

产品说明

分析说明

Assay (GC, area%): ≥ 99.0 % (a/a)
Density (d 20 °C/ 4 °C): 1.976 - 1.980
Identity (IR): passes test

基本信息

线性分子式Br(CH2)3Br
分子量201.89
MDL编号MFCD00000255
EC索引号203-690-3

产品性质

蒸汽压2.6 hPa ( 20 ℃)
质量水平200
测定≥99.0% (GC)
效能315 mg/kg LD50, oral (Rat)
bp166-168 ℃/1013 hPa
mp-34 ℃
转变温度flash point 54 ℃
密度1.98 g/cm3 at 20 ℃
储存温度2-30℃
InChI1S/C3H6Br2/c4-2-1-3-5/h1-3H2
InChI keyVEFLKXRACNJHOV-UHFFFAOYSA-N

安全信息

象形图GHS02GHS07GHS09
警示用语:Warning
危险声明H226 - H302 - H315 - H411
预防措施声明P210 - P233 - P240 - P273 - P301 + P312 - P303 + P361 + P353
危险分类Acute Tox. 4 Oral - Aquatic Chronic 2 - Flam. Liq. 3 - Skin Irrit. 2
储存分类代码3 - Flammable liquids
WGKWGK 2
闪点(F)129.2 °F - closed cup
闪点(C)54 ℃ - closed cup
991586Amethyst1,3-Dibromopropane99%, 用于合成40元/25G;   60元/100G;   174元/500G;   694元/2.5KG;   咨询

基本信息

分子式C3H6Br2
分子量201.89
熔点-34
沸点167
闪点56
密度1.989
MDL编码MFCD00000255
Beilstein635662
Merck14,9713
EINECS 编号203-690-3

安全信息

图形或危害标志
提示语Warning
危险说明H226
H302
H315
H319
H411
防范说明P211
P273
P281
P305+P351+P338
P370+P378
UN号码1993
危险分类3
包装等级III
WGK2
RTECSTX8575000
TSCA
003830Fluorochem1,3-Dibromopropane98%440元/25g;   572元/100g;   1650元/500g;   咨询

基本信息

CAS Number109-64-8
MDL NumberMFCD00000255
Boiling Point167℃
Melting Point-34℃
Density1.989

安全信息

图形或危害标志
危险性说明 H226: Flammable liquid and vapour.
H302: Harmful if swallowed.
H315: Causes skin irritation.
H412: Harmful to aquatic life with long lasting effects.
防范说明 P210: Keep away from – No smoking.
P233: Keep container tightly closed.
P240: Ground/bond container and receiving equipment.
P241: Use explosion-proof ./ equipment.
P242: Use only non-sparking tools.
P243: Take precautionary measures against static discharge.
P264: Wash hands thoroughly after handling.
P270: Do not eat, drink or smoke when using this product.
P273: Avoid release to the environment.
P280: Wear .
P301 + P312: IF SWALLOWED: Call a POISON CENTER or doctor/physician if you feel unwell.
P302 + P352: IF ON SKIN: Wash with plenty of soap and water.
P303 + P361 + P353: IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower.
P321: Specific treatment (see . on this label).
P330: Rinse mouth.
P332 + P313: If skin irritation occurs: Get medical advice/ attention.
P362: Take off contaminated clothing and wash before reuse.
P370 + P378: In case of fire: Use CO2 for extinction.
P403 + P235: Store in a well-ventilated place. Keep cool.
P501: Dispose of contents/container to local regulations.
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